compared with those processed with a ball mill (Spex a model 8000, Spex Industries, Edison, NJ). Plant samples were processed prior to roller milling and ball milling (Spex a model 8000, Spex Industries, Edison, NJ) with a Wiley a mill (20-mesh sieve) for leaf and stem materials, a Stein a mill for corn grain, and a Buhler a mill for flour.
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Sample preparation greatly increases the accuracy of the analytical results and unlike other analytical techniques, XRF analysis does not require extensive sample preparation work. Sample preparation methods are inexpensive, straightforward, fast, easy to learn and automated.
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Essentially, ball milling process is advantageous to remove the functional groups and creates the defects in addition to in-plane defects . In the present case, we strongly believe that a deoxyge- - ... phase purity using BRUKER Pan analytical powder X-ray diffractometer (XRD) using CuKα radiation with a
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